HCID 22163148, compound → HCID 43217234, compound

HRID 1088508Notes

Reaction equation

HRID 1088508 reaction equation
[CH3:1][C:2](=[N:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]([O:18][CH2:19][CH3:20])=[O:17])=[CH:12][CH:11]=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>[Pd].C(O)C>[CH3:1][CH:2]([NH:9][C:10]1[CH:11]=[CH:12][C:13]([C:16]([O:18][CH2:19][CH3:20])=[O:17])=[CH:14][CH:15]=1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 1

HCID 22163148HCID 22163148, compound

Product 1

HCID 43217234HCID 43217234, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

N-(α-methyl benzylidene)-p-carbethoxyaniline (XI) prepared by the procedure described in example XXIIA was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent to give N-(α-methyl benzyl)-p-carbethoxy aniline (XII). XII had a m.p. of 88° C.

Sources & evidence

ORD record
ord-34d810bed6e740fc9914bf9826dc25d6
Source dataset
uspto-grants-1990_10
Patent number
US04962234

Reaction notes

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