反应详情

A mixture of p-acetyl-N-(α-methyl benzylidene) aniline (XXIII) (40 g) prepared by the procedure described in example XXIXA and aniline (20 ml) was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent. The crude product was crystallized from ethanol to give 1,4-Bis-(1-anilinoethyl) benzene (XXV). XXV had a melting point of 169°-170° C.

1. customprepared by the procedure
2. customThe crude product was crystallized from ethanol