HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 1-(p-Dodecylanilino)-1,2,3,4-tetrahydronaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | N-(1,2,3,4-tetrahydronaphthylidene) aniline | HCID 11183633 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 1-(p-Dodecylanilino)-1,2,3,4-tetrahydronaphthalene | HCID 13037714 | — |
Reaction Steps
N-(1,2,3,4-tetrahydronaphthylidene) aniline (XXVI) (38 g) prepared as described in example XXXIA was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent. The crude product was crystallized from ethanol to give 1-(p-dodecylanilino)-1,2,3,4-tetrahydronaphthalene (XXVII). XXVII had a melting point of 34° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-f3fdc5945ac042beb85f594dac709a55 |
| Source note | uspto-grants-1990_10 |