Ethylene → tert-Amylbenzene

HRID 1088531Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1088531
[C:1]1([CH:7]([CH3:9])[CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:10]=[CH2:11]>>[C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)([CH2:10][CH3:11])([CH3:9])[CH3:8]

Komponenten

3

Edukt 2

HCID 6325EthyleneHCID 7406Cumene

Produkt 1

HCID 16295tert-Amylbenzene

Reaktionsbedingungen

Temperatur
160 °C

Versuchsvorschrift

In a 600 ml autoclave equipped with a magnetic stirrer, Solid Base A (0.45 g) and cumene (240 g) were charged under nitrogen, heated to 160° C. while stirring at 1,000 rpm and then reacted at the same temperature for 3 hours while supplying ethylene gas under pressure of 10 kg/cm2G. to produce tert.-amylbenzene (hereinafter referred to as "TAB").

Aufarbeitung

  1. customIn a 600 ml autoclave equipped with a magnetic stirrer
  2. customreacted at the same temperature for 3 hours

Quellen und Nachweise

ORD-Eintrag
ord-c6f6a67515fd4f49ac05b327653c4715
Quelldatensatz
uspto-grants-1990_10
Patentnummer
US04962254

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