Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | 4-Methoxy-alpha-toluenethiol | HCID 80407 | — |
| Product | HCID 53731568 | HCID 53731568 | — |
Reaction Steps
2.78 ml of epichlorohydrin and 2.78 ml of p-methoxybenzylmercaptan were heated with stirring at 120 to 130° C. for three hours. After cooling, the product was purified by column chromatography using 100 g of silica gel and benzene as an eluent to obtain 1.44 g of the objective compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04962202 |
|---|
| Source dataset | uspto-grants-1990_10 |
|---|
| ORD ID | ord-627bac4c69cc48ee8a9509c72000ee5e |
|---|
| Source note | uspto-grants-1990_10 |
|---|
