HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 15008680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-(2-Bromo-4-nitrophenyl)-2,3,3,3-tetrafluoro-2-(trifluoromethyl)propanamide | HCID 163755 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 15008680 | HCID 15008680 | 70% |
Reaction Steps
2'-Bromo-4'-nitro-2,3,3,3-tetrafluoro-2-(trifluoromethyl)propionanilide was reacted with methyl iodide, in acetone and in the presence of potassium carbonate, yielding N-methyl-2'-bromo-4'-nitro-2,3,3,3-tetrafluoro-2-(trifluoromethyl)propionanilide, an oil, yield 70% (>99% branched isomer).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962284 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-f55f15dd43e84910953823d075e161fb |
| Source note | uspto-grants-1990_10 |