HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1088583Generated: November 1, 2026
Chlorosulfonyl isocyanate → HCID 15616167, compound
https://huagongshe.com/reaction/1088583
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Reactant | HCID 11229285 | HCID 11229285 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15616167 | HCID 15616167 | — |
Reaction Steps
A solution of 3.7 g (0.026 mole) of chlorosulfonylisocyanate in 25 ml of absolute toluene are added dropwise to a solution of 4.8 g (0.025 mole) of allyl 3-methylsalicylate in 25 ml of absolute toluene, at 25° C. When the dropwise addition is complete, the temperature is increased slowly to 110° C., and the mixture is refluxed for 6 hours. The mixture is cooled and the solvent is removed on a rotary evaporator. The yellow oil remaining (7.5 g 100% of theory) is employed without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04963180 |
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| Source dataset | uspto-grants-1990_10 |
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| ORD ID | ord-2da8b3d6df6f46eaaf5fcd659ddfef57 |
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| Source note | uspto-grants-1990_10 |
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