HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-morpholinocarbonyl-L-phenylalanine benzyl ester → CP 84364
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-morpholinocarbonyl-L-phenylalanine benzyl ester | HCID 14478228 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | CP 84364 | HCID 664657 | 94,4% |
Reaktionsschritte
A solution of N-morpholinocarbonyl-L-phenylalanine benzyl ester (1.43 g) in methanol (20 ml) was hydrogenated over 10% palladium on carbon (150 mg) at 3 atmospheric pressure of hydrogen for 1 hour. The solution was filtered and concentrated in vacuo to give N-morpholinocarbonyl-L-phenylalanine (1.02 g) as an amorphous powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04963530 |
| Quelldatensatz | uspto-grants-1990_10 |
| ORD ID | ord-14ba90aef92248cb8d0b54e1cd080a1a |
| Quellennotiz | uspto-grants-1990_10 |