HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178514025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | O-benzylglycine toluene-p-sulphonate | HCID 6451311 | — |
| Reactant | 4-Methylbenzene-1-sulfonic acid--benzyl beta-alaninate (1/1) | HCID 13502100 | — |
| Reactant | HCID 178503853 | HCID 178503853 | — |
| Reactant | HCID 178521271 | HCID 178521271 | — |
| Product | HCID 178514025 | HCID 178514025 | — |
Reaction Steps
The reactions described in Reference Example 10 (1) and (2) were carried out using glycine benzyl ester p-toluenesulfonate in lieu of β-alanine benzyl ester p-toluenesulfonate to prepare 1-benzyloxycarbonylmethyl-1H-tetrazole-5-thiol, which was then converted with alcoholic ammonia into the captioned compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963542 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-a8072a790ac7414eaeaeb17d25d64cc4 |
| Source note | uspto-grants-1990_10 |