HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propylpent-4-enal → 2-Propylpentanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propylpent-4-enal | HCID 3018523 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-Propylpentanal | HCID 87560 | — |
Reaction Steps
A Parr hydrogenation bottle was charged with 10% palladium on carbon (0.1 equivalent) and ethyl acetate. A solution of 2-propylpent 4 enal, prepared as in Example 5, in ethyl acetate was added. The mixture was hydrogenated at 300N/m2 hydrogen in a Parr hydrogenation apparatus at room temperature until hydrogen uptake ceased. The catalyst was removed by filtration through celite. The filtrate was concentrated to give the desired product as a colorless oil. The product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04963557 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-346b3ce8d2ff4b18a02f7558503cc7fe |
| Source note | uspto-grants-1990_10 |