Water → HCID 22161771, compound

Participants

Reaction Steps

4-oxo-8-t-butyldimethylsilyloxymethyl-1-ethyl-1,2,3,4-tetrahydroquinoline (2.17 g) was dissolved in methanol (20 ml). To this solution was added sodium borohydride (0.26 g) at room temperature, and the mixture was stirred for 10 minutes. Water was added to the reaction mixture and the solvent was distilled off to give 8-t-butyldimethylsilyloxymethyl-4-hydroxy-1-ethyl-1,2,3,4-tetrahydroquinoline (2.30 g).

Provenance & Evidence