Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Stearoyl chloride | HCID 8212 | — |
| Reactant | HCID 53849680 | HCID 53849680 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 54006570 | HCID 54006570 | 17% |
Reaction Steps
A solution containing 2.0 g of the product obtained in Example 8 and 10.0 g of stearoyl chloride in 10 ml of dioxane was stirred and heated for 18 h at 90° C. After cooling petroleum ether was added and the product was filtered. Recrystallization from dichloromethane-petroleum ether yielded 0.64 g (17%) of the desired product desired, m.p. 112°-118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04963590 |
|---|
| Source dataset | uspto-grants-1990_10 |
|---|
| ORD ID | ord-0b157b67eccf43ad85ddfdb462aaf87a |
|---|
| Source note | uspto-grants-1990_10 |
|---|
