HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1088930Generated: October 31, 2026
2-Naphthalenecarboxaldehyde → 2-Naphthalenecarboxaldehyde, oxime
https://huagongshe.com/reaction/1088930
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Naphthalenecarboxaldehyde | HCID 6201 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Naphthalenecarboxaldehyde, oxime | HCID 592789 | 98.2% |
Reaction Steps
To a mixture of 7.8 g of 2-naphthalaldehyde and 7.1 ml of triethylamine in 100 ml of methylene chloride was added 3.54 g of hydroxylamine hydrochloride and the mixture heated at 35° C. for three hours. The organic reaction solvent was washed with water, dried and concentrated to give 8.4 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04963689 |
|---|
| Source dataset | uspto-grants-1990_10 |
|---|
| ORD ID | ord-68afda6e83ed4db4837418f5a9d1bbe4 |
|---|
| Source note | uspto-grants-1990_10 |
|---|
