Sodium Hydroxide → HCID 23705008, compound

HRID 1089073Notes

Reaction equation

HRID 1089073 reaction equation
[C:1]1([C:7]2[N:15]([CH3:16])[C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[CH:13][C:12](=[O:23])[C:8]=2[C:9]([OH:11])=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Na+:25]>CO>[C:1]1([C:7]2[N:15]([CH3:16])[C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[CH:13][C:12](=[O:23])[C:8]=2[C:9]([O-:11])=[O:10])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1.[Na+:25]

Participants

4

Reactant 2

HCID 14798Sodium Hydroxide2×HCID 14075370HCID 14075370, compound

Product 1

HCID 23705008HCID 23705008, compoundYield 94.4%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.73 gms of 2,6-diphenyl-1-methyl-4-oxonicotinic acid was suspended in 50 mls of dry methanol. 0.25 gms of NaOH was added. After the carboxylic acid and the NaOH dissolved the solvent was removed yielding 1.75 gms of sodium 2,6-diphenyl-1-methyl-4-oxonicotinate as a glassy solid.

Workup

  1. customwas removed

Sources & evidence

ORD record
ord-c423d05f9d914bd49df652648827a5e0
Source dataset
uspto-grants-1990_10
Patent number
US04964896

Reaction notes

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