HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone, 3-(nitromethyl)- → 3-(Aminomethyl)cyclohexan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone, 3-(nitromethyl)- | HCID 10920766 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 3-(Aminomethyl)cyclohexan-1-ol | HCID 23009844 | 24.5% |
Reaction Steps
37.2 g of 3-(nitromethyl)cyclohexanone are reduced with lithium aluminum hydride in analogy to the procedure for Example 2. In this way 7.5 g (24.5% of theory) of viscous oily 3-(aminomethyl)cyclohexanol are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04965258 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-90693dba20754d7eae681cb2e6c1e23d |
| Source note | uspto-grants-1990_10 |