Sodium Hydroxide → HCID 22160420, compound

HRID 1089130Notes

Reaction equation

HRID 1089130 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][CH2:9][C:10]([OH:12])=[O:11])=[CH:4][CH:3]=1.[CH2:13]([O:16][C:17](Cl)=[O:18])[CH:14]=[CH2:15].[OH-:20].[Na+]>>[CH2:13]([O:16][C:17]([NH:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]([C:17]([O:16][CH2:13][CH:14]=[CH2:15])=[O:20])[CH2:9][C:10]([OH:12])=[O:11])=[CH:4][CH:3]=1)=[O:18])[CH:14]=[CH2:15]

Participants

4

Reactant 3

HCID 14798Sodium HydroxideHCID 18052Allyl chloroformateHCID 13628314HCID 13628314, compound

Product 1

HCID 22160420HCID 22160420, compound

Procedure

Analogously to Example 6, 3.1 g of N-(4-aminophenyl)-glycine are converted with 4.97 ml of chloroformic acid allyl ester and sodium hydroxide solution into the title compound.

Sources & evidence

ORD record
ord-07f97ad5866743f68eac170cb8f5e350
Source dataset
uspto-grants-1990_10
Patent number
US04965260

Reaction notes

Loading…