N,N-Diethylbenzamide → HCID 15132484, compound

HRID 1089190Notes

Reaction equation

[CH2:1]([N:3]([CH2:12][CH3:13])[C:4](=[O:11])[C:5]1[CH:10]=[CH:9][CH:8]=CC=1)[CH3:2].N1CC[S:17]CC1.C1(C(Cl)=O)CCC1>>[CH:5]1([C:4]([N:3]2[CH2:1][CH2:2][S:17][CH2:13][CH2:12]2)=[O:11])[CH2:10][CH2:9][CH2:8]1

Participants

Reactant 3

HCID 15542N,N-Diethylbenzamide

HCID 67164Thiomorpholine

HCID 78705Cyclobutanecarbonyl chloride

Product 1

HCID 15132484HCID 15132484, compound

Procedure

The product of Example 42 was followed using thiomorpholine and cyclobutanecarbonyl chloride giving the desired product as a solid, mp 39°-40° C.

Sources & evidence

ORD record: ord-e01ed039ba8c4e50876c40a3b122b62d
Source dataset: uspto-grants-1990_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04965284

Reaction notes

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