化工社化工社 化学情報印刷レポート · 研究参考用
N-Trimethylsilyl-N-methylacetamide → 1-Methyl-1-(N-methylacetamido)silacyclobutane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Trimethylsilyl-N-methylacetamide | HCID 81953 | — |
| 反応物 | Silacyclobutane, 1-chloro-1-methyl- | HCID 137554 | — |
| 生成物 | 1-Methyl-1-(N-methylacetamido)silacyclobutane | HCID 15065924 | — |
反応手順
To 30.02 g 1-chloro-1-methylsilacyclobutane was added 36.10 g N-methyl-N-(trimethylsilyl)acetamide. The reaction products were fractionally distilled. The title compound was isolated as a clear, colorless fluid with a boiling point of 68°-76° C. at 3.6 mm Hg. The yield was 31.56 g (86%). The product was identified by NMR and mass spectroscopy.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04965367 |
| 出典データセット | uspto-grants-1990_10 |
| ORD ID | ord-1298a41f10a8426ba6037a47b4d89388 |
| 出典メモ | uspto-grants-1990_10 |