HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 14834718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Magnesium | HCID 5462224 | — |
| Reactant | HCID 14834717 | HCID 14834717 | — |
| Reactant | HCID 53973114 | HCID 53973114 | — |
| Product | HCID 14834718 | HCID 14834718 | 80% |
Reaction Steps
(4, ##STR16## R'=H, m=8) When 16.5 g (0.049 mole) of 3-hydroxy-12-cyclohexyltridecanoic acid ethylester, 20.6 g (0.17 mole) of allyl bromide and 24.3 g (0.20 mole) of magnesium was reacted as described for the preparation of -allyl-4,6-dihydroxyheptadec-1-ene, 14.9 g of a yellow oil was isolated in 80% yield which was used without purification; δ (CDCl3) 1.28(m,CH2) and 4.90-6.2(m,CH=CH2)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04965373 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-54d1aa5099cc446cb851c9b7c9a3b160 |
| Source note | uspto-grants-1990_10 |