HCID 10802198, compound → HCID 86744314, compound

HRID 1089338Notes

Reaction equation

HRID 1089338 reaction equation
[F:1][C:2]1[C:15]([F:16])=[CH:14][C:5]([C:6]([CH2:8][C:9]([O:11][CH2:12][CH3:13])=[O:10])=[O:7])=[C:4]([N+:17]([O-:19])=[O:18])[CH:3]=1.[CH2:20]([O:22][CH:23]([O-])[O-])[CH3:21]>C(O)(=O)C>[F:1][C:2]1[C:15]([F:16])=[CH:14][C:5]([C:6]([C:8](=[CH:23][O:22][CH2:20][CH3:21])[C:9]([O:11][CH2:12][CH3:13])=[O:10])=[O:7])=[C:4]([N+:17]([O-:19])=[O:18])[CH:3]=1

Participants

4

Reactant 2

HCID 10802198HCID 10802198, compoundHCID 53630039Ethylorthoformate

Product 1

HCID 86744314HCID 86744314, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

To 3 ml of acetic acid anhydrous were added 3 g (0.01 mol) of ethyl 4,5-difluoro-2-nitrobenzoylacetate and 2.44 g (0.016 mol) of ethylorthoformate.

Sources & evidence

ORD record
ord-cc83c5761d3e4cf0b4c3b1c6cec109fc
Source dataset
uspto-grants-1990_10
Patent number
US04965396

Reaction notes

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