1-Dodecanethiol → Dibutyltinbis(lauryl mercaptide)

HRID 1089383Notes

Reaction equation

HRID 1089383 reaction equation
[CH2:1]([Sn:5](=O)[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].[CH2:11]([SH:23])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>O>[CH2:1]([Sn:5]([CH2:6][CH2:7][CH2:8][CH3:9])([S:23][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[S:23][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 81951-DodecanethiolHCID 61221Dibutyltin oxide

Product 1

HCID 9561614Dibutyltinbis(lauryl mercaptide)

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

This compound was prepared from di-n-butyltin-oxide and 1 dodecanethiol by azeotropic removal of water using the method described in U.S. Pat. No. 2,648,650. All spectroscopic and analytical data were consistent with the proposed structure.

Sources & evidence

ORD record
ord-e579b006595e43b38ac36f487f52a63e
Source dataset
uspto-grants-1990_10
Patent number
US04966678

Reaction notes

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