HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-(1H-Imidazol-1-yl)-4-[2-[4-[(methylsulfonyl)amino]phenyl]acetyl]-3,4,5,6-tetrahydro-2H-1,7,4-benzodioxazonine → N-[4-[2-[9-(1H-Imidazol-1-yl)-3,4,5,6-tetrahydro-2H-1,7,4-benzodioxazonin-4-yl]ethyl]phenyl]methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-(1H-Imidazol-1-yl)-4-[2-[4-[(methylsulfonyl)amino]phenyl]acetyl]-3,4,5,6-tetrahydro-2H-1,7,4-benzodioxazonine | HCID 14856365 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | N-[4-[2-[9-(1H-Imidazol-1-yl)-3,4,5,6-tetrahydro-2H-1,7,4-benzodioxazonin-4-yl]ethyl]phenyl]methanesulfonamide | HCID 14856372 | — |
Reaction Steps
In a manner similar to example 8, react 9-(1H-imidazol-1-yl)-4-[2-[4-[(methylsulfonyl)amino]phenyl]acetyl]-3,4,5,6-tetrahydro-2H-1,7,4-benzodioxazonine with lithium aluminum hydride to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04966967 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-7e25810f3f53406a8016b356a3c82ce2 |
| Source note | uspto-grants-1990_10 |