Thionyl Chloride → HCID 19915522, compound

HRID 1089643Notes

Reaction equation

HRID 1089643 reaction equation
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].[C:14](OCCC)(=O)[C:15]1C=CC(C([O-])=O)=CC=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:14][CH3:15]

Participants

5

Reactant 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046, compoundHCID 23693908Potassium Monopropyl Terephthalate

Product 1

HCID 19915522HCID 19915522, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

This compound was prepared by the procedure described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monopropyl terephthalate (49.0g, 0.20 mole), thionyl chloride (29.8g, 0.25 mole) and 100 ml of toluene. The product was used without further purification.

Workup

  1. customThis compound was prepared by the procedure
  2. customThe product was used without further purification

Sources & evidence

ORD record
ord-ac7eb9e4db084883b32afbccc60fb5aa
Source dataset
uspto-grants-1992_01
Patent number
US05078907

Reaction notes

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