化工社化工社 化学情報印刷レポート · 研究参考用
Toluene → HCID 23693905、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Dibutyl terephthalate | HCID 16066 | — |
| 反応物 | 1,4-Benzenedicarboxylic acid, 1-methyl ester, potassium salt (1:1) | HCID 23683753 | — |
| 溶媒 | 1-Butanol | HCID 263 | — |
| 生成物 | HCID 23693905 | HCID 23693905 | 96% |
反応手順
This compound was prepared by the procedure described for potassium monomethyl terephthalate. Typical reagent levels were as follows: dibutyl terephthalate (10.0 g, 0.036 mole), potassium hydroxide (2.1 g, 0.036 mole), 50 ml of toluene and 20 ml of 1-butanol. After workup 9.4 g was recovered which represented a 96% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05078907 |
| 出典データセット | uspto-grants-1992_01 |
| ORD ID | ord-b90880285938405d8c622f2524386ee4 |
| 出典メモ | uspto-grants-1992_01 |