Thionyl Chloride → HCID 19915516, compound

HRID 1089646Notes

Reaction equation

HRID 1089646 reaction equation
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].[C:14](OCCCC)(=O)[C:15]1C=CC(C([O-])=O)=C[CH:16]=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:14][CH2:15][CH3:16]

Participants

5

Reactant 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046, compoundHCID 23693905Potassium Monobutyl Terephthalate

Product 1

HCID 19915516HCID 19915516, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

This compound was prepared by the procedure described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monobutyl terephthalate (10.0 g, 0.0384 mole), thionyl chloride (4.57, 0.0384 mole) and 40 ml of toluene. The yield of product was 8.5 g (92%). This material was used without further purification.

Workup

  1. customThis compound was prepared by the procedure
  2. customThis material was used without further purification

Sources & evidence

ORD record
ord-93af8425e7774440b21e6142f5d1b490
Source dataset
uspto-grants-1992_01
Patent number
US05078907

Reaction notes

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