HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hexanol → 1,4-Benzenedicarboxylic acid, 1-methyl ester, potassium salt (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hexanol | HCID 8103 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Dihexyl terephthalate | HCID 519527 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1,4-Benzenedicarboxylic acid, 1-methyl ester, potassium salt (1:1) | HCID 23683753 | — |
Reaction Steps
Typical reagent levels were as follows: dihexyl terephthalate (33.5 g, 0.10 mole), potassium hydroxide (5.6 g, 0.10 mole), 100 ml of toluene and 20 ml of 1-hexanol. After workup 20.2g (70%) of product was recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05078907 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-cf7e5e903a6647c694d5ca44036477cf |
| Source note | uspto-grants-1992_01 |