HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → Monohexyl Terephthaloyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22057046 | HCID 22057046 | — |
| Reactant | Potassium monohexyl terephthalate | HCID 23693907 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Monohexyl Terephthaloyl Chloride | HCID 19915510 | — |
Reaction Steps
This compound was prepared by the method described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monohexyl terephthalate (18.6 g, 0.64 mole), thionyl chloride (9.21 g, 0.774 mole) and 100 ml of toluene. The product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05078907 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-5ebe672c30364d6da854725a7ce28276 |
| Source note | uspto-grants-1992_01 |