HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanide → 2-(2,6-Dimethylpiperidino)amino-3-phenoxypropionitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | Phenoxyacetaldehyde | HCID 75033 | — |
| Reactant | 2,6-Dimethyl-1-piperidylamine | HCID 123482 | — |
| Product | 2-(2,6-Dimethylpiperidino)amino-3-phenoxypropionitrile | HCID 19915654 | 76.2% |
Reaction Steps
12.8 g of 1-amino-2,6-dimethylpiperidine, 5.4 g of sodium cyanide and 15.0 g of phenoxyacetaldehyde are reacted analogously to 8a). 20.8 g of 2-(2,6-dimethylpiperidino)amino-3-phenoxypropionitrile are obtained, which are employed in the following step without further purification
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05079244 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-6488102a1b7b4334bf2b2615994185af |
| Source note | uspto-grants-1992_01 |