HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 19915693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 19915704 | HCID 19915704 | — |
| Product | HCID 19915693 | HCID 19915693 | — |
Reaction Steps
Also isolated by chromatography was [(3-oxo-1-cyclohepten-1-yl)amino]-1-methyl-1H-indole -3-carbonitrile (D17) (1.30 g, 20%) Rf 0.19 (SiO2, 2:1 dichloromethane:ethyl acetate). This intermediate could be converted to the title compound (E16) using a procedure similar to that described in Description 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05079246 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-9abda4ee741d405ebdd60a41bbf46ba7 |
| Source note | uspto-grants-1992_01 |