HCID 14645091, compound → HCID 14645099, compound

HRID 1089696Notes

Reaction equation

HRID 1089696 reaction equation
[CH3:1][N:2]([CH2:14][CH2:15][S:16][C:17]1[CH:22]=[CH:21][C:20]([N+:23]([O-])=O)=[CH:19][CH:18]=1)[CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][C:8]([N+:11]([O-])=O)=[CH:7][CH:6]=1>[Ni]>[NH2:23][C:20]1[CH:19]=[CH:18][C:17]([S:16][CH2:15][CH2:14][N:2]([CH2:3][CH2:4][C:5]2[CH:6]=[CH:7][C:8]([NH2:11])=[CH:9][CH:10]=2)[CH3:1])=[CH:22][CH:21]=1

Participants

3

Reactant 1

HCID 14645091HCID 14645091, compound

Product 1

HCID 14645099HCID 14645099, compound

Reagents, catalysts & solvents 1

HCID 935NickelCatalyst

Procedure

The title compound was prepared by the hydrogenation of 2-[N-methyl-N-(4-nitrophenethyl)amino]-1-(4-nitrophenylthio)ethane over Raney nickel according to the procedure of Example 7(B).

Sources & evidence

ORD record
ord-dc21f0db28cd4ec29e4427b17e06fb19
Source dataset
uspto-grants-1992_01
Patent number
US05079248

Reaction notes

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