HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → 4-{4-[2-Chloroethoxy]benzoyl}morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 4-(2-chloroethoxy)benzoyl Chloride | HCID 11074871 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-{4-[2-Chloroethoxy]benzoyl}morpholine | HCID 19915729 | — |
Reaction Steps
4-(2-Chloroethoxy)benzoyl chloride (5.0 g) was dissolved in dry methylene chloride and stirred while cooling to 0°. Morpholine (4.0 g) was added dropwise and the mixture was stirred at room temperature for 2 days. The resultant colourless solid was filtered off and the liquors allowed to stand from which the title compound crystallised (5.5 g), m.p. 102°-104°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05079248 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-8e850304df9d4f539f10dfc4c73051f1 |
| Source note | uspto-grants-1992_01 |