1H-Imidazole-1-propanamine → HCID 10155797, compound

HRID 1089744Notes

Reaction equation

HRID 1089744 reaction equation
[C:1]1([CH2:7][N:8]2[C:16]3[C:11]4[C:12](=[CH:17][CH:18]=[CH:19][C:10]=4[C:9]2=S)[CH:13]=[CH:14][CH:15]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N:21]1([CH2:26][CH2:27][CH2:28][NH2:29])[CH:25]=[CH:24][N:23]=[CH:22]1>C(O)C>[C:1]1([CH2:7][N:8]2[C:16]3[C:11]4[C:12](=[CH:17][CH:18]=[CH:19][C:10]=4[C:9]2=[N:29][CH2:28][CH2:27][CH2:26][N:21]2[CH:25]=[CH:24][N:23]=[CH:22]2)[CH:13]=[CH:14][CH:15]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 787361H-Imidazole-1-propanamineHCID 15023412HCID 15023412, compound

Product 1

HCID 10155797HCID 10155797, compoundYield 66.3%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 3.0 g 1-(phenylmethyl)benz[cd]indole-2(1H)-thione (Cc), 1.34 g of 1H-imidazole-1-propaneamine, 10.0 ml ethyl alcohol, and 3.5 g of mercuric acetate is reacted as described in Example 3, giving 2.6 g of the desired product, mp. 90°-93° C.

Workup

  1. customis reacted

Sources & evidence

ORD record
ord-cad43596118d4bda877ebd066f6efd74
Source dataset
uspto-grants-1992_01
Patent number
US05079247

Reaction notes

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