1H-Imidazole-1-propanamine → HCID 15023429, compound

HRID 1089745Notes

Reaction equation

HRID 1089745 reaction equation
[C:1]1([CH:7]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[N:8]2[C:16]3[C:11]4[C:12](=[CH:17][CH:18]=[CH:19][C:10]=4[C:9]2=S)[CH:13]=[CH:14][CH:15]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N:27]1([CH2:32][CH2:33][CH2:34][NH2:35])[CH:31]=[CH:30][N:29]=[CH:28]1>C(O)C>[C:1]1([CH:7]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[N:8]2[C:16]3[C:11]4[C:12](=[CH:17][CH:18]=[CH:19][C:10]=4[C:9]2=[N:35][CH2:34][CH2:33][CH2:32][N:27]2[CH:31]=[CH:30][N:29]=[CH:28]2)[CH:13]=[CH:14][CH:15]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 787361H-Imidazole-1-propanamineHCID 15023413HCID 15023413, compound

Product 1

HCID 15023429HCID 15023429, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 1.0 g of 1-(diphenylmethyl)benz[cd]indole-2(1H)-thione (Cd), 0.35 g of 1H-imidazole-1-propanamine, 20 ml ethyl alcohol and 0.91 g of mercuric acetate is reacted as described in Example 3, giving the desired product, mp. 142°-143° C.

Workup

  1. customis reacted

Sources & evidence

ORD record
ord-0ae0126b845d4b99907f894200ac1550
Source dataset
uspto-grants-1992_01
Patent number
US05079247

Reaction notes

Loading…