1H-Imidazole-1-propanamine → HCID 10157594, compound

HRID 1089748Notes

Reaction equation

HRID 1089748 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:9][N:10]2[C:18]3[C:13]4[C:14](=[CH:19][CH:20]=[CH:21][C:12]=4[C:11]2=S)[CH:15]=[CH:16][CH:17]=3)[CH:6]=[CH:7][CH:8]=1.[N:23]1([CH2:28][CH2:29][CH2:30][NH2:31])[CH:27]=[CH:26][N:25]=[CH:24]1>C(O)C>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:9][N:10]2[C:18]3[C:13]4[C:14](=[CH:19][CH:20]=[CH:21][C:12]=4[C:11]2=[N:31][CH2:30][CH2:29][CH2:28][N:23]2[CH:27]=[CH:26][N:25]=[CH:24]2)[CH:15]=[CH:16][CH:17]=3)[CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 2

HCID 787361H-Imidazole-1-propanamineHCID 15023420HCID 15023420, compound

Product 1

HCID 10157594HCID 10157594, compoundYield 80.1%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 2.5 g of 1-[(3-methoxyphenyl)methyl]benz[cd]indole-2(1H)-thione (Ck), 1.1 g of 1H-imidazole-1-propanamine, 200 ml ethyl alcohol, and 2.6 g of mercuric acetate is reacted as described in Example 3, giving 2.6 g of the desired product, mp. 95°-96° C.

Workup

  1. customis reacted

Sources & evidence

ORD record
ord-edf7465be35d4135882716301bba9e66
Source dataset
uspto-grants-1992_01
Patent number
US05079247

Reaction notes

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