HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 15692974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19765264 | HCID 19765264 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15692974 | HCID 15692974 | — |
Reaction Steps
73 g of the carboxylic acid from Example c and 80 g of thionyl chloride in 200 ml of toluene are refluxed in the presence of a little dimethylformamide until the evolution of gas is complete. The crude carbonyl chloride which remains in quantitative yield after evaporation is directly reacted further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05080708 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-76edd10be85f48de9fc388c943ede731 |
| Source note | uspto-grants-1992_01 |