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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1090071Generated: October 31, 2026

Dimethylformamide dimethyl acetal → HCID 54199707, compound

https://huagongshe.com/reaction/1090071

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamide dimethyl acetalHCID 78373—
Reactant(2-Methyl-3-nitrophenyl)(naphthalen-1-yl)methanoneHCID 14535917—
SolventDimethylformamideHCID 6228—
ProductHCID 54199707HCID 54199707—

Reaction Steps

Following a procedure similar to that described in Preparation 2A above, 57 g (0.195 mole) of 2-methyl-3-(1-naphthylcarbonyl)nitrobenzene and 103 ml (0.784 mole) of DMF dimethyl acetal in 300 ml of DMF was heated under reflux for seventeen hours and then taken to dryness to give 2-(2-dimethylaminoethenyl)-3-(1-naphthylcarbonyl)nitrobenzene as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05081122
Source datasetuspto-grants-1992_01
ORD IDord-4b875be34ad849c29f8e4907171a62aa
Source noteuspto-grants-1992_01