HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1090093Generated: November 2, 2026
5-Chloro-2-nitrobenzoic acid → 5-Chloro-2-nitrobenzoyl chloride
https://huagongshe.com/reaction/1090093
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 5-Chloro-2-nitrobenzoyl chloride | HCID 2723685 | — |
Reaction Steps
A mixture of 80.6 g of 5-chloro-2-nitrobenzoic acid and 58.2 ml of thionyl chloride is heated at 90° C. for 2 hours. The excess thionyl chloride is then distilled off in vacuo. 87.1 g of 5-chloro-2-nitrobenzoyl chloride are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05081125 |
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| Source dataset | uspto-grants-1992_01 |
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| ORD ID | ord-9f30e9b4dc0e490bba318a420a2f10b8 |
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| Source note | uspto-grants-1992_01 |
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