HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 14577476, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 19905249 | HCID 19905249 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14577476 | HCID 14577476 | — |
Reaction Steps
56.6 g (149 mmol) of 2-{[1-(phenylmethyl)-4-piperidyl]methyl}-2,3-dihydro-1H-isoindole dihydrochloride, 300 ml of ethanol, 50 ml of water and 5 g of palladinized charcoal (10% palladium) are introduced into a Parr apparatus and a hydrogenolysis is performed under approximately 0.41 MPa for 9 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081128 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-5dcf58e017da428c83ac8228642df3b1 |
| Source note | uspto-grants-1992_01 |