HCID 15675231, compound → HCID 15675238, compound

HRID 1090127Notes

Reaction equation

HRID 1090127 reaction equation
[CH2:1]([O:8][C:9]1[C:10]([O:23][CH3:24])=[C:11]2[C:15](=[CH:16][CH:17]=1)[N:14](C(OC)=O)[CH:13]=[C:12]2[CH3:22])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(OC1C(OC)=CC=C2C=1C(C)=CN2)C1C=CC=CC=1>>[CH2:1]([O:8][C:9]1[C:10]([O:23][CH3:24])=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][CH:13]=[C:12]2[CH3:22])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 15675231HCID 15675231, compoundHCID 15675244HCID 15675244, compound

Product 1

HCID 15675238HCID 15675238, compoundYield 92%

Procedure

The 5-benzyloxy-4-methoxy-1-methoxycarbonyl-3-methylindole (4.5 g) was hydrolyzed in the same manner as in the preparation of 4-benzyloxy-5-methoxy-3-methylindole in Experimental Example 4 to give 5-benzyloxy-4-methoxy-3-methylindole (3.4 g).

Sources & evidence

ORD record
ord-2b2d1f93df154b058e740fed27fcb1cc
Source dataset
uspto-grants-1992_01
Patent number
US05081121

Reaction notes

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