Methyl 5-oxoheptanoate → HCID 15678773, compound

HRID 1090189Notes

Reaction equation

HRID 1090189 reaction equation
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][N:10]([C:12]2[CH:17]=[CH:16][C:15]([F:18])=[CH:14][CH:13]=2)N)=[CH:5][CH:4]=1.O=[C:20]([CH2:28][CH3:29])[CH2:21][CH2:22][CH2:23][C:24]([O:26]C)=[O:25]>C(O)(C)(C)C>[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][N:10]2[C:12]3[C:17](=[CH:16][C:15]([F:18])=[CH:14][CH:13]=3)[C:28]([CH3:29])=[C:20]2[CH2:21][CH2:22][CH2:23][C:24]([OH:26])=[O:25])=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 12576394Methyl 5-oxoheptanoateHCID 145912421-(p-Chlorobenzyl)-1-(4-fluorophenyl)hydrazine hydrochloride

Product 1

HCID 15678773HCID 15678773, compound

Reagents, catalysts & solvents 1

HCID 6386tert-ButanolSolvent

Procedure

Following the method of Example 2, but using 1-[(4-chlorophenyl)methyl]-1-(4-fluorophenyl)hydrazine hydrochloride and methyl 5-oxoheptanoate as the starting materials and tert-butanol as the solvent, the title compound was prepared.

Sources & evidence

ORD record
ord-f8b86131990f486087b810e0df584465
Source dataset
uspto-grants-1992_01
Patent number
US05081145

Reaction notes

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