HCID 12462596, compound → HCID 15678777, compound

HRID 1090190Notes

Reaction equation

HRID 1090190 reaction equation
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][N:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)N)=[CH:5][CH:4]=1.[CH3:20][CH:21]([C:27](=O)[CH2:28][CH3:29])[CH2:22][C:23]([O:25]C)=[O:24]>CO>[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][N:10]2[C:12]3[C:17](=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=3)[C:28]([CH3:29])=[C:27]2[CH:21]([CH3:20])[CH2:22][C:23]([OH:25])=[O:24])=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 12462596HCID 12462596, compoundHCID 189475691-(4-Chlorobenzyl)-1-(4-methoxyphenyl)hydrazine hydrochloride

Product 1

HCID 15678777HCID 15678777, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Following the method of Example 2, but using 1-[(4-chlorophenyl)methyl]-1-(4-methoxyphenyl)-hydrazine hydrochloride and methyl 3-methyl-4-oxohexanoate as the starting materials and methanol as the solvent, the title compound was prepared.

Sources & evidence

ORD record
ord-123a8a4fa9314010b38907d2229961e3
Source dataset
uspto-grants-1992_01
Patent number
US05081145

Reaction notes

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