Methyl 4-oxohexanoate → HCID 15678756, compound

HRID 1090196Notes

Reaction equation

HRID 1090196 reaction equation
[ClH:1].Cl[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH2:9][N:10]([C:12]1[CH:17]=[C:16]([Cl:18])[CH:15]=[C:14]([Cl:19])[CH:13]=1)N.O=[C:21]([CH2:28][CH3:29])[CH2:22][CH2:23][C:24]([O:26]C)=[O:25]>C(O)(C)(C)C>[Cl:19][C:14]1[CH:15]=[C:16]([Cl:18])[CH:17]=[C:12]2[C:13]=1[C:28]([CH3:29])=[C:21]([CH2:22][CH2:23][C:24]([OH:26])=[O:25])[N:10]2[CH2:9][C:4]1[CH:5]=[CH:6][C:7]([Cl:1])=[CH:8][CH:3]=1

Participants

4

Reactant 2

HCID 546293Methyl 4-oxohexanoateHCID 86745389HCID 86745389, compound

Product 1

HCID 15678756HCID 15678756, compound

Reagents, catalysts & solvents 1

HCID 6386tert-ButanolSolvent

Procedure

Following the method of Example 2, but using 1-[1-(chlorophenyl)methyl-1-(3,5-dichlorophenyl) hydrazine hydrochloride and methyl 4-oxohexanoate as the starting materials, in t-butanol as solvent, the title compound was prepared.

Sources & evidence

ORD record
ord-75fda334eda44e01a525456ed5de63e5
Source dataset
uspto-grants-1992_01
Patent number
US05081145

Reaction notes

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