HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2,2-dimethyl-4-oxohexanoate → 3-[1-(4-nitrobenzyl)-5-methoxy-3-methyl-1H-indol-2-yl]-2,2-dimethyl propanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2,2-dimethyl-4-oxohexanoate | HCID 13164740 | — |
| Reactant | (4-Nitrophenyl)methyl-1-(4-methoxyphenyl) hydrazine hydrochloride | HCID 70472787 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | 3-[1-(4-nitrobenzyl)-5-methoxy-3-methyl-1H-indol-2-yl]-2,2-dimethyl propanoic acid | HCID 15678811 | — |
Reaction Steps
Following the method of Example 2, but using 1-[(4-nitrophenyl)methyl-1-(4-methoxyphenyl) hydrazine hydrochloride and methyl 2,2-dimethyl-4-oxo-hexanoate as the starting materials and tert-butanol as the solvent, the title compound was prepared.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081145 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-194aa907561a488a9bcb9b67b8c72082 |
| Source note | uspto-grants-1992_01 |