HCID 13198406, compound → HCID 15678817, compound

HRID 1090209Notes

Reaction equation

HRID 1090209 reaction equation
Cl.[CH3:2][S:3][C:4]1[CH:20]=[CH:19][C:7]([CH2:8][N:9]([C:11]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=2)N)=[CH:6][CH:5]=1.C[O:22][C:23](=[O:32])[CH2:24][CH:25]([CH3:31])[CH2:26][C:27](=O)[CH2:28][CH3:29]>C(O)(C)(C)C>[CH3:2][S:3][C:4]1[CH:20]=[CH:19][C:7]([CH2:8][N:9]2[C:11]3[C:16](=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=3)[C:28]([CH3:29])=[C:27]2[CH2:26][CH:25]([CH3:31])[CH2:24][C:23]([OH:32])=[O:22])=[CH:6][CH:5]=1

Participants

4

Reactant 2

HCID 13198406HCID 13198406, compoundHCID 19914752HCID 19914752, compound

Product 1

HCID 15678817HCID 15678817, compound

Reagents, catalysts & solvents 1

HCID 6386tert-ButanolSolvent

Procedure

Following the method of Example 2, but using 1-[4-methylthiobenzyl]-1-[4-methoxyphenyl]hydrazine hydrochloride and methyl-3-methyl-5-oxoheptanoate as starting materials, in t-butanol as solvent, the title compound was prepared

Sources & evidence

ORD record
ord-e96b9d2f48f04edda891398097fc4b37
Source dataset
uspto-grants-1992_01
Patent number
US05081145

Reaction notes

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