HRID1090212

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID13952862

3-(1H-Imidazol-1-yl)butan-1-amine

C7H13N3

HCID178527759

未命名化合物

PRODUCTS

生成物

结构：CC(CCNC1=Nc2ccc(Br)c3cccc1c23)n1ccnc1

HCID178448831

未命名化合物

收率 41.3%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

A mixture of 5.2 g of 6-bromo-benz(cd)indole2-thiol, 2.8 g of 3-(1H-imidazol-l-yl)butanamine, 6.6 g of mercuric acetate and 100 ml of dry p-dioxane was reacted as described in Example 1, giving 3.0 g of the desired product, mp 240° C.-241° C.

WORKUP

后处理

customwas reacted