HRID1090214

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID78736

1H-Imidazole-1-propanamine

C6H11N3

结构：CN(C)S(=O)(=O)c1ccc2c3c(cccc13)C(=S)N2

HCID19914607

未命名化合物

PRODUCTS

生成物

结构：CN(C)S(=O)(=O)c1ccc2c3c(cccc13)C(NCCCn1ccnc1)=N2

HCID178486128

未命名化合物

收率 41.2%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A mixture of 5.0 g of 1,2-dihydro-N,N-dimethyl-2-thioxobenz(cd)indole-6-sulfonamide, 2.3 g of 3-(1H-imidazol-l-yl)propanamine, 100 ml of ethanol and 5.4 g of mercuric acetate was reacted as described in Example 1, giving 2.7 g of the desired product, mp 199° C.-201° C.

WORKUP

后处理

customwas reacted