反应详情

A mixture of 2.8 g of 10-(1H-imidazol-l-yl)decanamine, dihydrochloride was treated with 2 ml of 10N sodium hydroxide in an ethanol-water mixture giving the base derivative. To this base was added 25 ml of ethanol, 2.33 g of 6-bromo-benz(cd)indole-2-thiol and 3.0 g of mercuric acetate. The procedure of Example 1 was then followed, giving 2.8 g of the desired product, mp 115° C.-116° C.

1. customgiving the base derivative