反应详情

A mixture of 2.5 g of 12-(1H-imidazol-l-yl)dodecanamine, 1.9 g of benz(cd)indole-2-thiol, 3.4 g of mercuric acetate and 400 ml of ethanol was reacted as described in Example 1. The crude product was purified by dissolved it in chloroform and chromatographing it on a silica gel column, eluting with 10% methanol in chloroform giving 490 mg of the desired product, mp 95° C.-97° C.

1. customwas reacted
2. customThe crude product was purified
3. dissolutionby dissolved it in chloroform
4. washchromatographing it on a silica gel column, eluting with 10% methanol in chloroform giving 490 mg of the desired product, mp 95° C.-97° C.