Phenyl isocyanate → HCID 15034987, compound

Participants

Reaction Steps

A solution of 2.7 g of N-(3-(1H-imidazol-1-yl)propyl)benz(cd)indol-2-amine (free base of the compound of Example 1) was dissolved in 50 ml of dichloromethane, and the solution then treated with 2.4 grams of phenylisocyanate. The mixture was stirred at room temperature overnight and then washed with 50 ml of saturated NaCHO3 solution. The dichloromethane layer was dried over MgSO4. Removal of the dichloromethane in vacuo left 3.7 grams of the desired compound, melting at 240° C.-250° C. with decomposition.

Provenance & Evidence