1H-Imidazole-1-propanamine → HCID 178504648, compound

HRID 1090242Notes

Reaction equation

HRID 1090242 reaction equation
[CH3:1][S:2]([C:5]1[C:6]2[C:7]3[C:11](=[CH:12][CH:13]=1)[N:10]=[C:9](S)[C:8]=3[CH:15]=[CH:16][CH:17]=2)(=[O:4])=[O:3].[N:18]1([CH2:23][CH2:24][CH2:25][NH2:26])[CH:22]=[CH:21][N:20]=[CH:19]1>C(O)C>[N:18]1([CH2:23][CH2:24][CH2:25][NH:26][C:9]2[C:8]3[CH:15]=[CH:16][CH:17]=[C:6]4[C:7]=3[C:11](=[CH:12][CH:13]=[C:5]4[S:2]([CH3:1])(=[O:4])=[O:3])[N:10]=2)[CH:22]=[CH:21][N:20]=[CH:19]1

Participants

4

Reactant 2

HCID 787361H-Imidazole-1-propanamineHCID 178504649HCID 178504649, compound

Product 1

HCID 178504648HCID 178504648, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The reaction of molecular equivalents of 6-methylsulfonylbenz(cd)indol-2-thiol, 3-(1H-imidazol-1-yl)propanamine, mercuric acetate, and sufficient refluxing ethanol to permit stirring, by the procedure of Example 55 gives the title compound.

Sources & evidence

ORD record
ord-7a769a87c34b4157bf4d43f30bf35b2b
Source dataset
uspto-grants-1992_01
Patent number
US05081131

Reaction notes

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